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1 article(s) from Seyler, Helga

Controlled synthesis of poly(3-hexylthiophene) in continuous flow

Helga Seyler,
Jegadesan Subbiah,
David J. Jones,
Andrew B. Holmes and
Wallace W. H. Wong

Beilstein J. Org. Chem. 2013, 9, 1492–1500, doi:10.3762/bjoc.9.170

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Graphical Abstract

Scheme 1: (a) Preparation of thiophene Grignard monomer and synthesis of P3HT by Kumada catalyst transfer pol...

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Figure 1: Plot of number-average molecular weight, M_n, versus monomer–catalyst ratio [M]₀/[I]₀ for batch and ...

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Figure 2: MALDI mass spectrum of low-molecular-weight preparation (GPC, M_n = 6.2 kg/mol) of P3HT in continuou...

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Figure 3: Plot of number-average molecular weight, M_n, versus monomer–catalyst ratio [M]₀/[I]₀ for batch and ...

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Scheme 2: Schematic representation of the telescoped preparation of P3HT in a flow reactor.

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Figure 4: ¹H NMR (CDCl₃, 500 MHz) spectra of P3HT samples prepared in (a) flow and (b) batch show comparable ...

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Figure 5: (a) Schematic diagram of the photovoltaic device geometry and (b) J–V curves of BHJ solar cells wit...

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Published 25 Jul 2013

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